{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"建立了谷物类饲料中10种雄性激素、11种孕激素、10种糖皮质激素、5种雌性激素以及5种<span style=\"color:red\">二</span><span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span><span style=\"color:red\">内酯</span>类药物的液相色谱-串联质谱(LC-MS/MS)检测方法.均质样品经乙酸乙酯提取,以改良的QuEChERS吸附剂分散于提取液中实现快速净化.采用C18色谱柱(150 mm×2.1 mm,3.0 μm)分离,分别在正、负电喷雾串联质谱多反应监测模式下检测.在优化条件下,41种化合物在5.0～200.0μg/kg含量范围内有良好的线性相关性,相关系数均不低于0.99,定量限(S/N≥10)为0.123～2.72μg/kg.在5、40、200μg/kg或10、40、200μg/kg 3个添加水平下,豆粕类饲料中各化合物的回收率为70.3％～118.1％,相对标准偏差(RSD)为0.82％～19.5％；玉米类饲料中各化合物的回收率为76.1％～122.8％,RSD为1.3％～15.0％.该方法简便、快速、准确,可用于谷物类饲料中雄性激素、孕激素、糖皮质激素、雌性激素以及<span style=\"color:red\">二</span><span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span><span style=\"color:red\">内酯</span>类激素的筛查和测定.","authors":[{"authorName":"张毅","id":"062c6a46-b3fa-4a92-80fe-292ce7cc9c76","originalAuthorName":"张毅"},{"authorName":"蓝芳","id":"1f224144-1b40-42c2-a1a5-d54d5a5078ed","originalAuthorName":"蓝芳"},{"authorName":"张峰","id":"c404ab70-cd4d-4312-8349-f333d4e7b6c8","originalAuthorName":"张峰"},{"authorName":"沈金灿","id":"4da27b74-8e0f-4283-9361-468ca97af215","originalAuthorName":"沈金灿"},{"authorName":"储晓刚","id":"60d1f239-d8ac-44ae-a1bc-eed61046a583","originalAuthorName":"储晓刚"}],"doi":"10.3724/SP.J.1123.2011.00523","fpage":"523","id":"d1f9f794-f2c5-4e6c-b61c-7e455c23ec99","issue":"6","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"48ebc635-03b0-4b36-a908-94e66a350ffd","keyword":"液相色谱-串联质谱","originalKeyword":"液相色谱-串联质谱"},{"id":"8ace6fc8-c999-44d2-a17d-f21ba9627fa0","keyword":"雄性激素","originalKeyword":"雄性激素"},{"id":"97ee5176-1a21-4533-b0a5-e64d802f4d61","keyword":"孕激素","originalKeyword":"孕激素"},{"id":"f73e9257-2851-4bd4-922c-e677b6776e41","keyword":"糖皮质激素","originalKeyword":"糖皮质激素"},{"id":"10f246d7-47f8-4083-be60-ac5071e760ea","keyword":"雌性激素","originalKeyword":"雌性激素"},{"id":"1a5fc862-9afb-4292-bd5a-11036a6828e2","keyword":"<span style=\"color:red\">二</span><span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span><span style=\"color:red\">内酯</span>","originalKeyword":"二羟基苯甲酸内酯"},{"id":"0d85bb37-c3a5-4e84-bbc1-b27c54f9cf52","keyword":"谷物类饲料","originalKeyword":"谷物类饲料"}],"language":"zh","publisherId":"sp201106011","title":"液相色谱-串联质谱法测定谷物类饲料中的41种激素","volume":"29","year":"2011"},{"abstractinfo":"以<span style=\"color:red\">二</span><span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>和硫酸铜为原料通过反应沉淀法制备纳米<span style=\"color:red\">二</span><span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>铜催化剂.采用TEM、XRD、TG、IR等手段对样品进行了分析和表征,结果表明,不同溶剂洗涤影响最终粒子形状,乙醇溶剂洗涤处理得到<span style=\"color:red\">二</span><span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>铜球形粒子,平均粒径20～25nm.纯水处理后得到<span style=\"color:red\">二</span><span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>铜片状晶体.","authors":[{"authorName":"李裕","id":"7b41da6e-c7bf-4c1f-95dc-129c43db855a","originalAuthorName":"李裕"},{"authorName":"刘有智","id":"2f2fa2e7-6430-430a-9c5e-8ca5d6f16d65","originalAuthorName":"刘有智"},{"authorName":"郭雨","id":"a044cdcf-660c-4f5d-ac88-eb69f363ea32","originalAuthorName":"郭雨"}],"doi":"","fpage":"1681","id":"da8d8029-23d1-4ffa-8f95-b3983a4d9a9c","issue":"10","journal":{"abbrevTitle":"GNCL","coverImgSrc":"journal/img/cover/GNCL.jpg","id":"33","issnPpub":"1001-9731","publisherId":"GNCL","title":"功能材料"},"keywords":[{"id":"dc28a010-6cca-4840-a1ce-7bf909b62c81","keyword":"<span style=\"color:red\">二</span><span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>铜","originalKeyword":"二羟基苯甲酸铜"},{"id":"c07c0837-71d9-466b-b05d-caee85c66c18","keyword":"反应沉淀法","originalKeyword":"反应沉淀法"},{"id":"7280ebf3-2273-4f4b-8c72-b61985cce434","keyword":"纳米催化剂","originalKeyword":"纳米催化剂"}],"language":"zh","publisherId":"gncl200610048","title":"<span style=\"color:red\">二</span><span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>铜纳米催化剂的制备","volume":"37","year":"2006"},{"abstractinfo":"以固载杂多酸盐TiSiW12O40/TiO2为多相催化剂,对以乙醇、丙醇、丁醇和对<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>为原料合成对<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>酯的反应条件进行了研究.实验表明:TiSiW12O40/TiO2是合成对<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>酯的良好催化剂,最佳反应条件为:醇酸摩尔比为4:1,催化剂用量为反应物料总量的2%,反应时间为2 h.上述条件下,对<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>乙酯的产率为87.5%,对<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>丙酯的产率为89.2%,对<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>丁酯的产率为91.1%.","authors":[{"authorName":"杨水金","id":"1069a798-ce37-4386-a45e-341325187e7e","originalAuthorName":"杨水金"},{"authorName":"梁永光","id":"eb71bd2a-f6b3-4db4-b131-d42fbfb2f2c9","originalAuthorName":"梁永光"},{"authorName":"孙聚堂","id":"877f155d-a804-4876-828d-3c5995f791df","originalAuthorName":"孙聚堂"}],"doi":"","fpage":"1033","id":"20f606d9-5f53-474c-8626-1b1beb9818ea","issue":"12","journal":{"abbrevTitle":"XYJSCLYGC","coverImgSrc":"journal/img/cover/XYJSCLYGC.jpg","id":"69","issnPpub":"1002-185X","publisherId":"XYJSCLYGC","title":"稀有金属材料与工程"},"keywords":[{"id":"97f22b1d-7b4c-4e52-8387-597f4fc8e5b1","keyword":"对<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>酯","originalKeyword":"对羟基苯甲酸酯"},{"id":"dc1b0e68-f586-4a29-a36a-f568f0573f58","keyword":"催化剂","originalKeyword":"催化剂"},{"id":"881142db-5d79-440b-9da7-59bd9e5d1621","keyword":"TiSiW12O40/TiO2","originalKeyword":"TiSiW12O40/TiO2"}],"language":"zh","publisherId":"xyjsclygc200312016","title":"对<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>酯的合成","volume":"32","year":"2003"},{"abstractinfo":"采用超声协助甲醇提取、固相萃取净化、气相色谱/选择离子质谱联用法,同时测定化妆品中8种邻苯<span style=\"color:red\">二甲酸</span>酯和4种对<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>酯.该方法线性范围广、重现性好、快速简便、干扰小.样品的加标回收率为80%～160%;含量检测的相对标准偏差小于10%;方法的检出限为0.1～5.0 μg/kg.用该方法对15种实际样品中的12种残留物进行定量检测,结果表明除了一种样品中不含待测物外,其余样品均检测到3～7种待测物.其中以对<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>甲酯、对<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>丙酯、邻苯<span style=\"color:red\">二甲酸</span>丙酯、邻苯<span style=\"color:red\">二甲酸</span>环己酯和邻苯<span style=\"color:red\">二甲酸</span>乙基庚基酯为主.","authors":[{"authorName":"沈昊宇","id":"c426d70a-92fb-4d84-af1a-04841ca7d388","originalAuthorName":"沈昊宇"},{"authorName":"应丽艳","id":"b794d6e0-a7b7-4841-893d-cdc94591fae3","originalAuthorName":"应丽艳"},{"authorName":"曹云峰","id":"b67d38af-f534-4b47-97f3-db21c1a8a6c0","originalAuthorName":"曹云峰"},{"authorName":"潘刚","id":"37ce31da-5590-461c-b99b-0978e3deb2a6","originalAuthorName":"潘刚"},{"authorName":"周鹿","id":"e55f370a-2d97-4efa-8571-8d5f9cb7a6ea","originalAuthorName":"周鹿"}],"doi":"10.3321/j.issn:1000-8713.2007.02.032","fpage":"272","id":"87a2968c-9342-491f-a104-6cfe8e34c01b","issue":"2","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"ce747f0b-3b3f-427b-b3a3-bc76ca5a6460","keyword":"气相色谱/质谱法","originalKeyword":"气相色谱/质谱法"},{"id":"2958a551-b2a9-4b8f-bfdf-0ffa6f715d1e","keyword":"固相萃取","originalKeyword":"固相萃取"},{"id":"e1db940c-6bd0-4fd4-b807-8996c4c890e0","keyword":"邻苯<span style=\"color:red\">二甲酸</span>酯","originalKeyword":"邻苯二甲酸酯"},{"id":"918b819c-fa5a-4172-a50e-423afa876f58","keyword":"对<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>酯","originalKeyword":"对羟基苯甲酸酯"},{"id":"1abb9b20-0411-4440-858d-622f5f6580b8","keyword":"化妆品","originalKeyword":"化妆品"}],"language":"zh","publisherId":"sp200702032","title":"固相萃取-气相色谱/质谱法同时测定化妆品中的邻苯<span style=\"color:red\">二甲酸</span>酯和对<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>酯","volume":"25","year":"2007"},{"abstractinfo":"基于在表面活性剂吐温40存在条件下,3,4-<span style=\"color:red\">二</span><span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>与铈(Ⅳ)在酸性介质中发生化学发光反应,建立了测定微量3,4-<span style=\"color:red\">二</span><span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>的化学发光分析法.该法测定3,4-<span style=\"color:red\">二</span><span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>的线性范围为8.0×10-7～1.0×10-4mol/L,检出限为5.0×10-7mol/L,相对标准偏差为3.0%(8.0×10-6mol/L3,4-<span style=\"color:red\">二</span><span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>,n=11).该法应用于测定淠河水中加入的3,4-<span style=\"color:red\">二</span><span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>,结果令人满意.","authors":[{"authorName":"谢成根","id":"69b4bdd4-b33b-442e-b22e-d2c204c3086d","originalAuthorName":"谢成根"},{"authorName":"李淮芬","id":"3e4e1e6c-f991-461d-a250-08452023249f","originalAuthorName":"李淮芬"}],"doi":"10.3969/j.issn.1000-7571.2004.03.006","fpage":"17","id":"27c4ee84-5fd1-459e-8870-b03a7fa0a5a7","issue":"3","journal":{"abbrevTitle":"YJFX","coverImgSrc":"journal/img/cover/YJFX.jpg","id":"71","issnPpub":"1000-7571","publisherId":"YJFX","title":"冶金分析   "},"keywords":[{"id":"9f847945-0b1b-41cc-b20c-98858626a21c","keyword":"化学发光","originalKeyword":"化学发光"},{"id":"ea610394-0dff-4f09-9091-3fe7476f1222","keyword":"铈(Ⅳ)","originalKeyword":"铈(Ⅳ)"},{"id":"d3445dfc-8693-4381-ae9a-02f35c2919ac","keyword":"3,4-<span style=\"color:red\">二</span><span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>","originalKeyword":"3,4-二羟基苯甲酸"},{"id":"eb33570c-5a09-4965-b5a2-7f30d5f7b545","keyword":"吐温40","originalKeyword":"吐温40"}],"language":"zh","publisherId":"yjfx200403006","title":"铈(Ⅳ)-3,4-<span style=\"color:red\">二</span><span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>-吐温40化学发光体系的研究及其应用","volume":"24","year":"2004"},{"abstractinfo":"在辣根过氧化物酶（HRP）／H2O2的催化作用下间苯<span style=\"color:red\">二</span>酚（RE）和3，5-<span style=\"color:red\">二</span><span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>（DBA）通过自由基共聚反应生成酚类共聚物，研究了RE和DBA的配比对共聚物鞣剂性能的影响，用FT—IR、1↑HNMR、13↑CNMR、GPC和UV等方法对酚类共聚物的分子结构进行了表征。水溶液中HRP／H2O2催化自由基聚合反应的显著特征是共聚物的相对分子质量容易控制，酚类聚合物苯环直接相连，结构内存在较大的共轭体系。应用结果表明酚类聚合物具有较好的鞣制效果，鞣制后的皮革收缩温度（T5）达到了78．6℃，复鞣皮革非常柔软丰满。","authors":[{"authorName":"吕生华","id":"2a2dbb31-fb54-4c77-8f18-101894cb3e29","originalAuthorName":"吕生华"},{"authorName":"刘晶晶","id":"699feed7-9ef9-4d3d-b41c-1c16beed4535","originalAuthorName":"刘晶晶"},{"authorName":"王飞","id":"6138e541-9d9d-4a02-ae29-55ca125f8321","originalAuthorName":"王飞"},{"authorName":"李芳","id":"bf2ea15b-2ee9-49f4-9ee1-523e9655c0fc","originalAuthorName":"李芳"},{"authorName":"张国运","id":"c46660a1-9d87-46e4-9727-2e3fa982fa8c","originalAuthorName":"张国运"},{"authorName":"胡静","id":"d0c2440d-93ce-480c-b8e9-7777e1ddf12c","originalAuthorName":"胡静"}],"doi":"","fpage":"2926","id":"86fb4856-9735-4675-9340-bb80e40427de","issue":"21","journal":{"abbrevTitle":"GNCL","coverImgSrc":"journal/img/cover/GNCL.jpg","id":"33","issnPpub":"1001-9731","publisherId":"GNCL","title":"功能材料"},"keywords":[{"id":"6d6f63c0-96cf-4475-b4ef-317c93ce427b","keyword":"辣根过氧化物酶","originalKeyword":"辣根过氧化物酶"},{"id":"10f215b5-e991-4146-9063-4bea01f2a586","keyword":"酚类共聚物","originalKeyword":"酚类共聚物"},{"id":"4fde88d4-8c28-49db-87d9-d78e38c62d2a","keyword":"自由基共聚合","originalKeyword":"自由基共聚合"},{"id":"e8c4b627-a320-49b4-a76d-3e47a697d54d","keyword":"鞣制机理","originalKeyword":"鞣制机理"}],"language":"zh","publisherId":"gncl201221010","title":"HRP／H2O2催化间苯<span style=\"color:red\">二</span>酚和3，5-<span style=\"color:red\">二</span><span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>的聚合及其结构与性能的关系","volume":"43","year":"2012"},{"abstractinfo":"应用溶胶-凝胶技术,通过在纳米SiO2微粒的形成过程中原位合成稀土有机配合物,制备了尺寸60～80 nm的铽(Ⅲ)与对<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>配合物掺杂的纳米SiO2微粒.在铽与对<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>配合物掺杂纳米SiO2微粒的水溶液中观察到了很强的绿色发光,这类稀土有机配合物掺杂的纳米SiO2微粒在生物荧光探测中有广泛的应用前景.","authors":[{"authorName":"邹永金","id":"77287649-c1ca-4053-a041-8d6064107417","originalAuthorName":"邹永金"},{"authorName":"王峰","id":"c6a28651-01d0-46a6-8a4c-228188bb75bf","originalAuthorName":"王峰"},{"authorName":"樊先平","id":"c3f95a32-20d4-400b-9994-ec0af687f3a2","originalAuthorName":"樊先平"}],"doi":"","fpage":"477","id":"71641ab8-a46f-4265-9e58-24e3f35fe5b5","issue":"z2","journal":{"abbrevTitle":"XYJSCLYGC","coverImgSrc":"journal/img/cover/XYJSCLYGC.jpg","id":"69","issnPpub":"1002-185X","publisherId":"XYJSCLYGC","title":"稀有金属材料与工程"},"keywords":[{"id":"2279ce51-e3f9-4fb9-a2a5-f7dec0f80ad6","keyword":"溶胶-凝胶技术","originalKeyword":"溶胶-凝胶技术"},{"id":"51bdb4cd-e8fc-4387-a331-260d11d645ba","keyword":"SiO2纳米颗粒","originalKeyword":"SiO2纳米颗粒"},{"id":"b52b5d12-ce9c-4e64-9afc-65bee32cd2b9","keyword":"稀土有机配合物","originalKeyword":"稀土有机配合物"},{"id":"a4f6f49a-9c2b-4903-ae11-3a16fe3f18c6","keyword":"发光","originalKeyword":"发光"}],"language":"zh","publisherId":"xyjsclygc2008z2126","title":"铽(Ⅲ)与对<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>配合物掺杂的纳米<span style=\"color:red\">二</span>氧化硅微粒的制备及发光性能","volume":"37","year":"2008"},{"abstractinfo":"在N2气保护下,3-甲酰基-4-<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>甲酯与环己<span style=\"color:red\">二</span>胺在无水乙醇中缩合反应合成了新型的Schiff碱配体N,N'-双(3-甲酰基-4-<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>甲酯)缩环己<span style=\"color:red\">二</span>胺,收率为66.7%.该配体与四水合醋酸锰在无水乙醇中反应,并经空气氧化、氯化锂处理得到Mn3+配合物;与三氯化铁、氯化镍在无水乙醇中配位分别得到Fe3+、Ni2+配合物.并通过红外光谱、核磁共振、元素分析等测试方法对配体和配合物结构进行了表征.","authors":[{"authorName":"张雅然","id":"425e1356-6b33-45e7-9eac-fe326cb164c4","originalAuthorName":"张雅然"},{"authorName":"赵继全","id":"1d0f362d-8d77-492f-8bf8-e29523ebf5fa","originalAuthorName":"赵继全"},{"authorName":"何乐芹","id":"e2b1a1c2-af46-4ad0-b8b5-051c8410f412","originalAuthorName":"何乐芹"},{"authorName":"张松梅","id":"ba38ecd1-0d16-45a4-a5d6-51c76fe1f554","originalAuthorName":"张松梅"},{"authorName":"吴伟鹏","id":"a01af52c-ea9b-4099-b5cf-334f6a3656b0","originalAuthorName":"吴伟鹏"}],"doi":"10.3969/j.issn.1000-0518.2006.04.026","fpage":"450","id":"821815e8-3f14-4b21-ad76-ede1df4d071f","issue":"4","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"42a88a91-17b3-4750-8133-f7df06b8fff8","keyword":"N,N'-双(甲酰基<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>甲酯)缩环己<span style=\"color:red\">二</span>胺","originalKeyword":"N,N'-双(甲酰基羟基苯甲酸甲酯)缩环己二胺"},{"id":"7800dda9-d668-4ab2-82c5-b699830375e4","keyword":"Schiff碱","originalKeyword":"Schiff碱"},{"id":"0aa4fa86-d866-4522-9344-533472cbce43","keyword":"金属配合物","originalKeyword":"金属配合物"}],"language":"zh","publisherId":"yyhx200604026","title":"N,N'-双(3-甲酰基-4-<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>甲酯)缩环己<span style=\"color:red\">二</span>胺Schiff碱过渡金属配合物的合成及表征","volume":"23","year":"2006"},{"abstractinfo":"建立了固相萃取-高效液相色谱(SPE-HPLC)同时测定水果和果酱中6种对<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>酯(对<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>甲酯、对<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>乙酯、对<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>异丙酯、对<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>丙酯、对<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>异丁酯和对<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>丁酯)含量的方法.经Oasis HLB固相萃取柱净化的样品采用HPLC分离,优化的色谱条件为采用Symmetry-C_(18)色谱柱分离,流动相为柠檬酸缓冲液-甲醇(体积比为48∶52),流速1.0 mL/min,检测波长258 nm,测定温度40 ℃.6种对<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>酯的线性范围为0.1～20.0 mg/L(r=0.999 9),回收率为82.8% ～115.5%,相对标准偏差为0.2% ～6.8%(n=6).对<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>甲酯、对<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>乙酯、对<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>异丙酯、对<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>丙酯的检出限(S/N=3)为0.1 mg/kg,定量限(S/N=10)为0.3 mg/kg;对<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>异丁酯和对<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>丁酯的检出限为0.2 mg/kg,定量限为0.6 mg/kg.该方法简便快速、结果准确、重现性好,可作为测定水果及果酱中多种对<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>酯的有效方法.","authors":[{"authorName":"陈皑","id":"c3ffb76d-42df-4b67-b108-f6cbeb76ac02","originalAuthorName":"陈皑"},{"authorName":"何乔桑","id":"1a2274f1-f790-495b-972b-bad220cb308c","originalAuthorName":"何乔桑"},{"authorName":"王萍亚","id":"48534198-0f7c-4ff5-a8e1-64b8ac4a5c39","originalAuthorName":"王萍亚"},{"authorName":"周勇","id":"1c8d3ce2-dcab-48f0-833f-6d232f4a48f9","originalAuthorName":"周勇"},{"authorName":"黄鹂","id":"0dbdb6c5-8e07-43f7-9f3c-303a0673c76c","originalAuthorName":"黄鹂"},{"authorName":"许镇坚","id":"f28b4bd5-0863-4885-bb9b-d9916cb058b8","originalAuthorName":"许镇坚"},{"authorName":"赵华","id":"c02e2f60-5190-4b9d-931e-97f1737b13dc","originalAuthorName":"赵华"},{"authorName":"张薇英","id":"414aa250-d004-40cf-b87b-9a07daff6595","originalAuthorName":"张薇英"}],"doi":"10.3321/j.issn:1000-8713.2009.06.013","fpage":"804","id":"378655d8-a917-4ab4-90b6-d3803ce4ded4","issue":"6","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"001a5d02-cf0b-4efb-90e1-d375a30706f0","keyword":"固相萃取","originalKeyword":"固相萃取"},{"id":"815b46fe-c1e9-4037-836c-a2e89335d5a2","keyword":"高效液相色谱法","originalKeyword":"高效液相色谱法"},{"id":"4b3eb7b3-b964-4077-86b7-6aad68cb78c1","keyword":"对<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>酯","originalKeyword":"对羟基苯甲酸酯"},{"id":"3158e9c9-33ef-44e5-aa68-676ac1d14880","keyword":"水果","originalKeyword":"水果"},{"id":"1b732430-5608-41ce-a602-c5d39d083e97","keyword":"果酱","originalKeyword":"果酱"}],"language":"zh","publisherId":"sp200906013","title":"固相萃取-高效液相色谱法测定水果和果酱中的6种对<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>酯","volume":"27","year":"2009"},{"abstractinfo":"采用十六烷基三甲基溴化铵(CTAB)为电渗流改性剂,考察了邻<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>、间<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>和对<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>在高效毛细管区带电泳模式下的分离行为,研究了缓冲液的pH和添加剂甲醇的用量对这3种同分异构体的分离、峰形和出峰顺序的影响,并据此优化了这3种异构体的分离条件.","authors":[{"authorName":"张强","id":"cbd7ee7d-3b04-4f3e-95ee-12d68f6c2176","originalAuthorName":"张强"}],"doi":"10.3321/j.issn:1000-8713.2001.03.007","fpage":"217","id":"7b18ed4f-98ae-46c4-b1b0-527e2b9f9ce6","issue":"3","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"729fa2b4-fe30-4e7b-a94a-17a6f7dd8ad0","keyword":"毛细管区带电泳","originalKeyword":"毛细管区带电泳"},{"id":"4ad9da4b-bc6e-4517-ae33-954fb5eabb9e","keyword":"邻<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>","originalKeyword":"邻羟基苯甲酸"},{"id":"781830a8-b58d-49b7-b4cf-3e1be29b8ee1","keyword":"间<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>","originalKeyword":"间羟基苯甲酸"},{"id":"7b6cef56-21a6-41f9-9dbb-61726f971cfa","keyword":"对<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>","originalKeyword":"对羟基苯甲酸"}],"language":"zh","publisherId":"sp200103007","title":"<span style=\"color:red\">羟基</span><span style=\"color:red\">苯甲酸</span>的3种异构体的毛细管区带电泳分离研究","volume":"19","year":"2001"}],"totalpage":3251,"totalrecord":32503}