{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"开展了<span style=\"color:red\">动物</span><span style=\"color:red\">内脏</span>中14种酞酸酯类(PAEs)环境激素残留的气相色谱-电子轰击离子源质谱(GC-EI/MS)分析方法的研究,优化与选择了<span style=\"color:red\">动物</span><span style=\"color:red\">内脏</span>样品的前处理条件.<span style=\"color:red\">动物</span><span style=\"color:red\">内脏</span>样品经正己烷-二氯甲烷(体积比为1∶1)混合提取剂超声提取、Florisil硅土固相萃取柱净化与乙酸乙酯-正己烷(体积比为2∶3)混合洗脱剂洗脱和浓缩后,以邻苯二甲酸二苯基酯(DPhP)为内标物,采用GC-EI/MS的选择离子检测方式(SIM)进行定性和定量分析.当猪肝样品的加标浓度水平为100,200,400 μg/kg时,加标回收率为60% ～110% ,相对标准偏差为0.8% ～10.3% .除邻苯二甲酸二甲氧基乙酯(DMEP)与邻苯二甲酸二(2-乙氧基乙基)酯(DEEP)的方法检出限(MDL)分别为3.30 μg/kg 与2.25 μg/kg外,其余12种PAEs的MDL均不大于1.74 μg/kg;线性范围为50.0～800.0 μg/kg,相关系数均大于 0.999 4.该分析方法已成功地应用于6种<span style=\"color:red\">动物</span><span style=\"color:red\">内脏</span>中14种痕量PAEs残留的分析.","authors":[{"authorName":"林竹光","id":"4eeeb717-a4dd-4591-8f73-ed79dbe3f282","originalAuthorName":"林竹光"},{"authorName":"孙若男","id":"e52b75a2-2a4c-4bfe-93ef-60973772832e","originalAuthorName":"孙若男"},{"authorName":"张莉莉","id":"2d30ce2a-b42e-47b1-982b-9f8057ce55d7","originalAuthorName":"张莉莉"},{"authorName":"邹西梅","id":"be6f6950-1411-4077-962a-75c05c91809c","originalAuthorName":"邹西梅"},{"authorName":"陈美瑜","id":"92ab1f8e-5e89-4ca5-8364-a3caa77c514f","originalAuthorName":"陈美瑜"},{"authorName":"涂逢樟","id":"71dc53f7-e8ed-4601-9052-75d10aaa0567","originalAuthorName":"涂逢樟"},{"authorName":"马玉","id":"dfd1db62-5b32-4da9-a4f5-d14166f2c1bc","originalAuthorName":"马玉"},{"authorName":"蒋文静","id":"4f5d6454-de0a-4605-80cc-ab76231bd9ce","originalAuthorName":"蒋文静"}],"doi":"10.3321/j.issn:1000-8713.2008.03.003","fpage":"280","id":"4972b176-680c-496c-9370-ce650428ecc7","issue":"3","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"029e7a13-dbe4-4845-a5e3-c0cdb06c8af6","keyword":"气相色谱-电子轰击离子源质谱法","originalKeyword":"气相色谱-电子轰击离子源质谱法"},{"id":"4bc332de-fdc3-4c55-9abe-077ed38f1fb8","keyword":"<span style=\"color:red\">动物</span><span style=\"color:red\">内脏</span>","originalKeyword":"动物内脏"},{"id":"19ebfa23-2b93-4a78-a479-1ce56ffb411c","keyword":"酞酸酯","originalKeyword":"酞酸酯"}],"language":"zh","publisherId":"sp200803003","title":"气相色谱-质谱法同时测定<span style=\"color:red\">动物</span><span style=\"color:red\">内脏</span>中的14种酞酸酯类环境激素残留","volume":"26","year":"2008"},{"abstractinfo":"取自蒙古国境内,自然放牧和喂食添加稀土饲料的羊,宰杀后,立即取出<span style=\"color:red\">内脏</span>,利用微波消解仪溶解样品,电感耦合等离子体质谱法测定其中的稀土元素.研究了稀土元素在心、肝、脾、胃、肾中的分布特征.结果表明,稀土总量∑REE0.31 μg/g ～ 4.59μg/g,平均为1.85 μg/g,轻重稀土比值在5.10～19.57之间,平均为11.88,由LREE/HREE值可以看出轻稀土含量明显高于重稀土,这可能与包头地区的稀土分布有关;用稀土饲料喂养的羊的<span style=\"color:red\">内脏</span>中的稀土含量明显优于自然放牧的,尤其是肝和肾;包头地区的稀土主要以轻稀土为主,只有少量的重稀土,但肝脏中Gd、Tb、Er通过稀土饲料喂养后,相对富集;肾脏中Gd、Tb、Dy、Er、Y通过稀土饲料喂养后,相对富集.","authors":[{"authorName":"张立锋","id":"9578ea78-39a0-4722-8f4a-c542fd4bd775","originalAuthorName":"张立锋"},{"authorName":"马嘉东","id":"a7d49040-fa94-4fe1-a724-74a40fee9599","originalAuthorName":"马嘉东"},{"authorName":"周凯红","id":"24042e91-58d7-406a-8854-762a41edb2a4","originalAuthorName":"周凯红"},{"authorName":"张翼明","id":"bc630053-730c-4b56-9607-8b1c850edd5c","originalAuthorName":"张翼明"}],"doi":"10.16533/J.CNKI.15-1099/TF.201606023","fpage":"134","id":"5f51cfbb-08d0-4731-9be1-ccff7f2b9af2","issue":"6","journal":{"abbrevTitle":"XT","coverImgSrc":"journal/img/cover/XT.jpg","id":"65","issnPpub":"1004-0277","publisherId":"XT","title":"稀土"},"keywords":[{"id":"37c5220b-9639-467c-b5ba-464453008552","keyword":"ICP-MS","originalKeyword":"ICP-MS"},{"id":"5db65a2e-25a4-43fb-99b8-1e671d7ed946","keyword":"羊体<span style=\"color:red\">内脏</span>","originalKeyword":"羊体内脏"},{"id":"b62cf963-f7af-4fbf-af72-bb53d5b22017","keyword":"稀土元素","originalKeyword":"稀土元素"}],"language":"zh","publisherId":"xitu201606023","title":"羊体<span style=\"color:red\">内脏</span>中稀土元素分布特征研究","volume":"37","year":"2016"},{"abstractinfo":"研究了鱼<span style=\"color:red\">内脏</span>水解液FVH和竹叶提取液BLE两种酸洗缓蚀剂分别对碳钢在HCl介质中的缓蚀作用及复配后的缓蚀效果。结果表明这两种缓蚀剂具有良好的协同缓蚀作用。","authors":[{"authorName":"张健","id":"122c52b5-cb61-497f-9c49-2e34e22b7cd6","originalAuthorName":"张健"},{"authorName":"雷海辉","id":"05127efc-3aa3-4a84-9485-357b7ef1bdff","originalAuthorName":"雷海辉"},{"authorName":"韦海强","id":"f2eaaa6d-7a92-4ebf-a305-fa7e16a73525","originalAuthorName":"韦海强"}],"categoryName":"|","doi":"","fpage":"86","id":"c403c8f2-88f8-468f-b647-3ebdd858ba3c","issue":"1","journal":{"abbrevTitle":"FSXB","coverImgSrc":"journal/img/cover/腐蚀学报封面.jpg","id":"24","issnPpub":"2667-2669","publisherId":"FSXB","title":"腐蚀学报（英文）"},"keywords":[{"id":"ec9f1fc4-3560-4d3e-b2bb-b202be68a014","keyword":"鱼<span style=\"color:red\">内脏</span>","originalKeyword":"鱼内脏"},{"id":"81628dd5-8376-4166-afad-f1143d0f095b","keyword":"null","originalKeyword":"null"},{"id":"790cb66f-43d2-498b-aa5e-1db17735f6dd","keyword":"null","originalKeyword":"null"},{"id":"7c77034f-e5e8-4b26-b62c-7e6573ddffbe","keyword":"null","originalKeyword":"null"}],"language":"zh","publisherId":"1002-6495_1996_1_13","title":"鱼<span style=\"color:red\">内脏</span>水解液(FVH)与竹叶提取液(BLE)在HCl介质中的协同缓蚀作用","volume":"8","year":"1996"},{"abstractinfo":"分别从凝胶强度、表观黏度和黏结强度分,探索了明胶、甘油、蔗糖、氯化钠共混对<span style=\"color:red\">动物</span>蛋白胶的性能影响.","authors":[{"authorName":"李光鹏","id":"bea2d00d-5b0a-4d56-a71e-7c742c09ae85","originalAuthorName":"李光鹏"},{"authorName":"陈惠娟","id":"b2f5aefa-8506-46bb-bd73-9737aa292508","originalAuthorName":"陈惠娟"},{"authorName":"史琴梅","id":"753091dd-c1f0-4d5f-9672-2da6192478f3","originalAuthorName":"史琴梅"},{"authorName":"向海燕","id":"0b73a41d-a757-442b-a74c-43c660cd1951","originalAuthorName":"向海燕"}],"doi":"","fpage":"33","id":"4c43b4ff-f7d8-4a35-bc8a-dfba016284ec","issue":"2","journal":{"abbrevTitle":"HCCLLHYYY","coverImgSrc":"journal/img/cover/HCCLLHYYY.jpg","id":"42","issnPpub":"1671-5381","publisherId":"HCCLLHYYY","title":"合成材料老化与应用"},"keywords":[{"id":"1070f528-c2bd-47b8-9714-1bfef1192e9e","keyword":"<span style=\"color:red\">动物</span>蛋白胶","originalKeyword":"动物蛋白胶"},{"id":"da4cbd75-e472-4844-b5ad-92c1b492be80","keyword":"共混","originalKeyword":"共混"},{"id":"a58e115a-f3b1-4437-98e3-2e7899611767","keyword":"改性","originalKeyword":"改性"}],"language":"zh","publisherId":"hccllhyyy201302009","title":"<span style=\"color:red\">动物</span>蛋白胶共混改性研究","volume":"42","year":"2013"},{"abstractinfo":"本文研究了硝酸铈对大白鼠<span style=\"color:red\">内脏</span>组织、大脑及骨骼肌中一氧化氮、一氧化氮合成酶的影响.结果显示,腹腔注射高浓度的稀土后,大鼠肝脏、心脏、肾脏、骨骼肌中一氧化氮、一氧化氮合成酶的水平明显增加,注射低浓度的稀土后,肝脏、肾脏内一氧化氮的量显著增加.提示稀土能够广泛影响机体一氧化氮、一氧化氮合酶的水平,一氧化氮有可能参与了稀土的中毒过程.","authors":[{"authorName":"杨维东","id":"b2f55d59-2080-4689-b2a8-741056802375","originalAuthorName":"杨维东"},{"authorName":"刘洁生","id":"04eccabe-2bff-4458-aac2-3de547dfec7c","originalAuthorName":"刘洁生"},{"authorName":"王艇","id":"cce4f204-d766-4034-9a9b-5ddca111db21","originalAuthorName":"王艇"},{"authorName":"雷衡毅","id":"aa9e9a60-f40a-452f-8191-11e7503544e9","originalAuthorName":"雷衡毅"},{"authorName":"杨燕生","id":"de858ddf-f9a6-4692-afb2-d439fcfe590d","originalAuthorName":"杨燕生"}],"doi":"10.3969/j.issn.1004-0277.2000.02.012","fpage":"46","id":"ab1de7d3-b82a-4474-9337-6f05390a0f38","issue":"2","journal":{"abbrevTitle":"XT","coverImgSrc":"journal/img/cover/XT.jpg","id":"65","issnPpub":"1004-0277","publisherId":"XT","title":"稀土"},"keywords":[{"id":"6e08e93c-1b88-44c0-9a08-4ccfeec952b3","keyword":"稀土","originalKeyword":"稀土"},{"id":"88784872-343e-47f2-9058-0eff7428df7c","keyword":"一氧化氮","originalKeyword":"一氧化氮"},{"id":"afd0f5aa-80ee-4bfd-8d54-b51b3fe9f366","keyword":"一氧化氮合成酶","originalKeyword":"一氧化氮合成酶"},{"id":"dd369d76-55f4-4cc5-bc93-ec0b1ea80eb3","keyword":"大鼠","originalKeyword":"大鼠"}],"language":"zh","publisherId":"xitu200002012","title":"Ce(NO3)3对大鼠<span style=\"color:red\">内脏</span>组织和大脑一氧化氮及合成酶的影响","volume":"21","year":"2000"},{"abstractinfo":"本文利用扫描电镜、电子探针等手段， 研究分析了生物玻璃涂层植入<span style=\"color:red\">动物</span>骨组织后， 涂层表面与骨界面的显微变化及元素分布生物实验结果， 羟脯氨酸和氨基已糖含量与骨折后羟脯氨酸和氨基已糖含量变化的趋势一致","authors":[{"authorName":"顾卫明","id":"d55ac87b-f737-4526-83ba-d7feb507cc4c","originalAuthorName":"顾卫明"},{"authorName":"黄炳堂","id":"d81c4e12-d344-48c4-a344-908729ab5c88","originalAuthorName":"黄炳堂"},{"authorName":"孙荆","id":"463bd1de-1f24-456b-bb4c-ded7b6e35437","originalAuthorName":"孙荆"},{"authorName":"钱伟君","id":"297ba26f-758e-4da0-b0a0-6005c6da98ae","originalAuthorName":"钱伟君"},{"authorName":"戴其昌","id":"1cd92af0-7603-42d8-b7f3-9fae73589cf7","originalAuthorName":"戴其昌"},{"authorName":"鲍贤鸿","id":"026adff0-331f-47ac-8bbd-a7694cf5c5fc","originalAuthorName":"鲍贤鸿"}],"categoryName":"|","doi":"","fpage":"640","id":"8b1f024a-4ad8-4abc-864d-7409a7b4a9c6","issue":"4","journal":{"abbrevTitle":"WJCLXB","coverImgSrc":"journal/img/cover/WJCLXB.jpg","id":"62","issnPpub":"1000-324X","publisherId":"WJCLXB","title":"无机材料学报"},"keywords":[{"id":"1b665aa6-8752-4798-a22c-aef12a771011","keyword":"生物玻璃","originalKeyword":"生物玻璃"},{"id":"46d3a3d6-f7ce-413b-8eab-673b1f5403a7","keyword":" implant","originalKeyword":" implant"},{"id":"6671c618-352d-4dcc-b347-14cc4937faf1","keyword":" biochemistry experiment","originalKeyword":" biochemistry experiment"},{"id":"fb0248bc-39d9-4570-b9b4-79eb38ad4027","keyword":"null","originalKeyword":"null"}],"language":"zh","publisherId":"1000-324X_1999_4_13","title":"生物玻璃涂层植入材料的<span style=\"color:red\">动物</span>实验研究","volume":"14","year":"1999"},{"abstractinfo":"将不同形态AZ31B镁合金植入实验<span style=\"color:red\">动物</span>(兔子)体内,并以钛合金作对照组,研究了镁合金对实验<span style=\"color:red\">动物</span>的影响及其在实验<span style=\"color:red\">动物</span>体内的降解行为.研究结果表明,镁合金植入2周后,植入物周围有骨痂生成;8周后生成成熟的骨组织.镁合金植入并未对<span style=\"color:red\">动物</span>机体的循环、免疫、泌尿系统产生负面影响,体内降解产物主要为钙镁磷灰石,可经肾脏代谢,血液中的镁离子浓度在正常值范围内波动.本实验研究证明,镁合金植入<span style=\"color:red\">动物</span>体内在早期阶段对<span style=\"color:red\">动物</span>是安全的,且有诱导机体新骨生成的作用.","authors":[{"authorName":"张广道","id":"8db74534-39be-4c74-998b-d153ddda80d0","originalAuthorName":"张广道"},{"authorName":"黄晶晶","id":"387e33fc-3bae-4ddb-a39b-6e5bf006e671","originalAuthorName":"黄晶晶"},{"authorName":"杨柯","id":"817ad6bc-b7fa-4b10-bad6-884ce36f3230","originalAuthorName":"杨柯"},{"authorName":"张炳春","id":"88e557ee-905c-4b27-a746-780f76302756","originalAuthorName":"张炳春"},{"authorName":"艾红军","id":"4d7177ff-0c59-49c7-aabd-ce0feaddae9e","originalAuthorName":"艾红军"}],"doi":"10.3321/j.issn:0412-1961.2007.11.012","fpage":"1186","id":"dac76171-c8d6-4f4d-b8b1-e928af67f1b3","issue":"11","journal":{"abbrevTitle":"JSXB","coverImgSrc":"journal/img/cover/JSXB.jpg","id":"48","issnPpub":"0412-1961","publisherId":"JSXB","title":"金属学报"},"keywords":[{"id":"8e402549-6967-42b2-997e-27b6be278301","keyword":"金属基生物材料","originalKeyword":"金属基生物材料"},{"id":"2e582d14-5dcc-4ad9-8613-209ea61268d2","keyword":"镁合金","originalKeyword":"镁合金"},{"id":"be43d889-a9f5-4e7f-a39f-a2c636f15ec4","keyword":"可吸收材料","originalKeyword":"可吸收材料"},{"id":"953f0c20-8174-4414-9b35-e19f4120d892","keyword":"骨","originalKeyword":"骨"}],"language":"zh","publisherId":"jsxb200711012","title":"<span style=\"color:red\">动物</span>体内植入镁合金的早期实验研究","volume":"43","year":"2007"},{"abstractinfo":"采用细胞学实验和<span style=\"color:red\">动物</span>实验方法对用于温热治疗肿瘤的钙铁硅铁磁体微晶玻璃进行生物活性研究。<span style=\"color:red\">动物</span>试验结果表明，试样对<span style=\"color:red\">动物</span>无明显毒性，对<span style=\"color:red\">动物</span>的生长也无任何不利影响。细胞学实验结果表明，试样的细胞生物活性良好。","authors":[{"authorName":"陈建华","id":"8b6d9873-8430-4518-9e43-ea2e960b4d78","originalAuthorName":"陈建华"},{"authorName":"宗卉","id":"cb986efc-1f39-4051-ac2b-419ceed9097c","originalAuthorName":"宗卉"},{"authorName":"马立新","id":"d0784810-a2bd-4234-a255-9d7681aba094","originalAuthorName":"马立新"},{"authorName":"杨南如","id":"43a4bf14-2c26-4ea4-8264-11980eb3d37e","originalAuthorName":"杨南如"}],"doi":"","fpage":"56","id":"bc9df166-3c98-444c-95df-608c7f578364","issue":"12","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"bcf0c693-fe34-4090-8250-7a334238e8f4","keyword":"铁磁体","originalKeyword":"铁磁体"},{"id":"7dced967-c9ad-49b4-9812-a3cc26d57e01","keyword":"微晶玻璃","originalKeyword":"微晶玻璃"},{"id":"6524afe3-ded4-4d24-b8d5-1fd37184e4cb","keyword":"生物活性","originalKeyword":"生物活性"}],"language":"zh","publisherId":"cldb200012018","title":"钙铁硅铁磁体微晶玻璃的细胞学及<span style=\"color:red\">动物</span>学实验研究","volume":"14","year":"2000"},{"abstractinfo":"研究了纯镁及表面改性纯镁样品植入<span style=\"color:red\">动物</span>骨组织后在镁-骨界面处的降解机制以及材料对周围骨组织的影响.选择纯系日本大耳白兔,于股骨处植入样品.术后1、5周后,取出样品制作半薄切片,进行光学显微镜、扫描电镜观察.研究发现,镁棒周围新生类骨组织沉积速度很快,说明镁的腐蚀降解并没有影响骨组织修复过程.结果表明,镁在降解期间安全性较高,有较好的组织相容性.","authors":[{"authorName":"黄晶晶","id":"84835426-c3a9-4dd5-bbe2-402c8dc33697","originalAuthorName":"黄晶晶"},{"authorName":"杨柯","id":"aecc0980-a7cb-4e06-b82f-a61ff59e8951","originalAuthorName":"杨柯"},{"authorName":"任伊宾","id":"4f9fb107-53ba-48ad-813f-32c37ae38213","originalAuthorName":"任伊宾"},{"authorName":"张炳春","id":"6cae02fb-9c16-44a1-a013-3d4be2bb6c83","originalAuthorName":"张炳春"},{"authorName":"于国宁","id":"85c26bb9-f4eb-4071-81ca-95d31d73b03c","originalAuthorName":"于国宁"},{"authorName":"蒋阅","id":"553cc086-b436-4cba-8136-8454c502e169","originalAuthorName":"蒋阅"}],"doi":"","fpage":"629","id":"da3aa3d2-22eb-446e-b837-36f23dae64ed","issue":"4","journal":{"abbrevTitle":"XYJSCLYGC","coverImgSrc":"journal/img/cover/XYJSCLYGC.jpg","id":"69","issnPpub":"1002-185X","publisherId":"XYJSCLYGC","title":"稀有金属材料与工程"},"keywords":[{"id":"d769036a-9656-4e19-bde8-3e772e24b461","keyword":"镁","originalKeyword":"镁"},{"id":"e5333f76-8630-4124-9fbd-f2a4ed4c8515","keyword":"降解","originalKeyword":"降解"},{"id":"0cd3f4c6-ad04-4b04-985f-8ddcdd56d56c","keyword":"骨","originalKeyword":"骨"},{"id":"8560d3da-7d17-43c4-9f77-ad0f80111410","keyword":"组织相容性","originalKeyword":"组织相容性"}],"language":"zh","publisherId":"xyjsclygc200804014","title":"镁植入<span style=\"color:red\">动物</span>体内的短期效果","volume":"37","year":"2008"},{"abstractinfo":"用电镜观察了土壤<span style=\"color:red\">动物</span>的典型体表形态,从理论上分析了土壤<span style=\"color:red\">动物</span>非光体表能降低体表润湿性及减少土壤粘附的机制.据此研制的触土部件仿生复合涂层,在磨料磨损条件下能有效地形成类似于土壤<span style=\"color:red\">动物</span>体表的非光滑形态,使其表面润湿性明显降低,具有减粘降阻的功能。","authors":[{"authorName":"贾贤","id":"fef4f1d0-a25f-422c-8cea-15a4bf64ec13","originalAuthorName":"贾贤"},{"authorName":"任露泉","id":"a9889d10-c4de-40c7-8523-e857c149b4d7","originalAuthorName":"任露泉"},{"authorName":"陈秉聪","id":"083695e9-2b62-4861-b282-36f40eaab5d6","originalAuthorName":"陈秉聪"}],"categoryName":"|","doi":"","fpage":"556","id":"390bfc97-0830-45a9-947c-d5a2a732a0ef","issue":"5","journal":{"abbrevTitle":"CLYJXB","coverImgSrc":"journal/img/cover/CLYJXB.jpg","id":"16","issnPpub":"1005-3093","publisherId":"CLYJXB","title":"材料研究学报"},"keywords":[{"id":"22c87bb4-6f18-4204-8563-1f447b6f49db","keyword":"仿生","originalKeyword":"仿生"},{"id":"e797edc1-b22d-435b-9cac-64b8ea571c4d","keyword":"null","originalKeyword":"null"},{"id":"801efaed-353a-4270-8a44-54f228b03778","keyword":"null","originalKeyword":"null"},{"id":"6aaf20df-04a0-4c9a-adf1-77a1f8e6e30a","keyword":"null","originalKeyword":"null"},{"id":"de48e9ab-df69-4aae-aded-d44eaef87b60","keyword":"null","originalKeyword":"null"}],"language":"zh","publisherId":"1005-3093_1996_5_2","title":"土壤<span style=\"color:red\">动物</span>体表及仿生复合涂层的润湿性","volume":"10","year":"1996"}],"totalpage":28,"totalrecord":276}